Bis(4-chlorobenzoic) anhydride - Names and Identifiers
Bis(4-chlorobenzoic) anhydride - Physico-chemical Properties
Molecular Formula | C14H8Cl2O3
|
Molar Mass | 295.12 |
Density | 1.401±0.06 g/cm3(Predicted) |
Melting Point | 193-194 °C(Solv: water (7732-18-5); acetone (67-64-1)) |
Boling Point | 248 °C(Press: 5 Torr) |
Flash Point | 182.5°C |
Solubility | Acetone (Slightly), Chloroform (Slightly) |
Vapor Presure | 6.63E-08mmHg at 25°C |
Appearance | Solid |
Color | White to Off-White |
Storage Condition | under inert gas (nitrogen or Argon) at 2-8°C |
Stability | Moisture Sensitive |
Refractive Index | 1.607 |
Bis(4-chlorobenzoic) anhydride - Risk and Safety
Hazard Symbols | T - Toxic
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Bis(4-chlorobenzoic) anhydride - Introduction
Bis (4-chorobenzoic) anhydride is an organic compound with the chemical formula C14H8Cl2O3. The following is a description of the properties, uses, preparation and safety information of the compound:
Nature:
- Bis(4-chlorobenzoic) anhydride is a white to pale yellow solid.
-Its melting point is about 147-150°C.
-It has lower solubility at room temperature and is easier to dissolve in non-polar solvents.
-It has a pungent smell.
Use:
- Bis(4-chlorobenzoic) anhydride is a commonly used organic synthesis intermediate that can be used to synthesize compounds with important biological activities.
-It can also be used as one of the precursors of fluorescent dyes, and has certain applications in the fields of optoelectronics and material science.
Preparation Method:
- Bis(4-chlorobenzoic) anhydride is mainly prepared by the anhydride reaction of 4-chlorobenzoic acid.
-A commonly used preparation method is to react excess 4-chlorobenzoic acid with anhydrous acetic acid or anhydrous thionyl chloride to produce Bis(4-chlorobenzoic) anhydride.
-The reaction needs to be carried out under an inert atmosphere, and the temperature and reaction time are controlled to increase the yield.
Safety Information:
- Bis(4-chlorobenzoic) anhydride is an organic compound and needs to be handled with care.
-It may have an irritating effect on the eyes, skin and respiratory system, so it is recommended to wear appropriate protective equipment during operation.
-Avoid inhaling dust, contact with skin and eyes.
-Keep away from fire and heat sources during use and storage, and maintain a well-ventilated environment.
-Disposal of waste in accordance with local regulations and do not dump.
Last Update:2024-04-10 22:29:15